Abstract
A study was made of the separation of mixtures of dimethyltryptamine, mescaline, psilocybin, ibogaine, and lysergic acid diethylamide, using both gas chromatography and thin-layer chromatography. Temperature-programmed gas chromatography of the trimethylsilyl derivatives gave excellent separations, as did thin-layer chromatography of the original compounds, using a dual-solvent method.